N-(3-Chloro­phen­yl)-4-methyl­benzene­sulfonamide

نویسندگان

  • B. Thimme Gowda
  • Sabine Foro
  • P. G. Nirmala
  • Hartmut Fuess
چکیده

In the title compound, C(13)H(12)ClNO(2)S, the conformation of the N-H bond is anti to the 3-chloro group in the aniline benzene ring. The dihedral angle between the two benzene rings is 73.7 (1)°. The crystal structure features inversion-related dimers linked by pairs of N-H⋯O hydrogen bonds.

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منابع مشابه

N-(2-Chloro­phen­yl)-4-methyl­benzene­sulfonamide

The mol-ecule of the title compound, C(13)H(12)ClNO(2)S, is bent at the S atom with a C-SO(2)-NH-C torsion angle of -54.8 (2)°. The dihedral angle between the two aromatic rings is 71.6 (1)°. An intra-molecular N-H⋯Cl hydrogen bond is observed. The crystal structure features inversion-related dimers formed by pairs of N-H⋯O hydrogen bonds.

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4-Chloro-N-(3-chloro­phen­yl)-2-methyl­benzene­sulfonamide

In the title compound, C(13)H(11)Cl(2)NO(2)S, the conformation of the N-H bond in the C-SO(2)-NH-C segment is anti to the meta-Cl atom on the aniline ring and syn to the ortho-methyl group on the sulfonyl-benzene ring. Furthermore, the torsion angle of the C-SO(2)-NH-C segment in the mol-ecule is 80.1 (3)°. The two benzene rings are tilted relative to each other by 70.9 (1)°. In the crystal, pa...

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4-Chloro-N-(2-chloro­phen­yl)-2-methyl­benzene­sulfonamide

In the crystal structure of the title compound, C(13)H(11)Cl(2)NO(2)S, the conformations of the N-C bond in the C-SO(2)-NH-C segment are trans and gauche with respect to the S=O bonds. The C-S(O(2))-N(H)-C torsion angle is 74.8 (4)°, indicating that the mol-ecule is bent at the S atom. In the crystal structure, inversion dimers linked by pairs of N-H⋯O hydrogen bonds occur. An intramolecular N-...

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4-Chloro-N-(4-chloro­phen­yl)-2-methyl­benzene­sulfonamide

In the title compound, C(13)H(11)Cl(2)NO(2)S, the conformations of the N-C bonds in the C-SO(2)-NH-C segment have gauche torsions with respect to the S=O bonds. Further, the conformation of the N-H bond is syn to the ortho-methyl group in the sulfonyl benzene ring. The torsion angle of the C-SO(2)-NH-C segment in the mol-ecule is 55.0 (2)°. The two benzene rings are tilted relative to each othe...

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3-(4-Chloro­phen­yl)-1-[(E)-1-(4-chloro­phen­yl)-2-(4-methyl­phenyl­sulfan­yl)ethen­yl]-4-(4-methyl­phenyl­sulfan­yl)-1H-pyrazole

In the title compound, C(31)H(24)Cl(2)N(2)S(2), the pyrazole ring adopts planar conformation with a maximum deviation of 0.002 (2) Å. The chloro-phenyl rings are twisted out of the plane of the pyrazole ring by 75.1 (1) and 39.5 (1)°. The crystal packing is controlled by weak intermolecular C-H⋯π interactions.

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عنوان ژورنال:

دوره 66  شماره 

صفحات  -

تاریخ انتشار 2010